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Objetivo: Testar a hipótese nula de que a orientação das ranhuras superficiais não influencia na vida em fadiga de fios de níquel-titânio (NiTi). Material e Métodos: Segmentos de fio de NiTi (Moreli, Sorocaba/SP, Brasil) medindo 30mm e com diâmetro de 0,40mm foram utilizados. As ranhuras foram criadas em relação à direção longitudinal, em 45 e 90 graus. O fio foi analisado sob microscopia eletrônica de varredura e a rugosidade, quantificada por interferometria. O número de ciclos para a fratura (NCF) foi determinado pelo teste de flexão rotativa. Resultados: A rugosidade entre os grupos de 45 e 90 graus apresentou diferenças estatisticamente significativas (p<0,05). O grupo sem ranhuras apresentou o maior NCF (p<0,05). O grupo com ranhuras em 45 graus apresentou maior NCF, em comparação ao grupo com 90 graus (p<0,05). Conclusões: A direção das ranhuras possui influência na vida em fadiga dos fios de NiTi. O NCF aumenta com a redução do ângulo das ranhuras em relação ao longo eixo do fio, independentemente da profundidade das ranhuras (AU).

Objective: this study tested the null hypothesis that the surface grooves orientation does not influence the NiTi wire cyclic fatigue. Material and methods: Segments of NiTi wire (Moreli, Sorocaba, Brazil) measuring 30mm and with a 0.40mm of diameter were used. Grooves were created in the longitudinal direction, at 45 degrees and 90 degrees. The wire was analyzed with SEM and the roughness was quantified by interferometry. The number of cycles until fracture (NCF) was determined by the cyclic fatigue test. Results: the roughness between 45 and 90 degrees groups presented differences (p<0.05). The group without grooves presented the highest NCF (p<0.05). The group with 45 degrees grooves presented better NCF in comparison to the group with 90 degrees (p<0.05). Conclusions: the direction of the grooves influences the fatigue life. The NCF increases with the reduction of the angle of the grooves in relation to the long axis, regardless of the depth of the grooves (AU).

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OBJECTIVES: To evaluate the cyclic fatigue resistance of Reciproc M-Wire R25 (VDW, Munich, Germany) and Reciproc R25 Blue instruments (VDW) driven by Direct® (VDW) contra-angle connected to an ordinary an air-driven motor or an electric motor and compare the results with those obtained by the Reciproc M-Wire R25 or Reciproc Blue R25 instruments driven by an electric torque-controlled motor using "RECIPROC ALL" preset program. MATERIALS AND METHODS: Thirty Reciproc M-Wire R25 (25/0.08v) and 30 Reciproc Blue R25 (25/0.08v) instruments were used. Cyclic fatigue resistance was tested measuring the time to fracture and the number of cycles to fracture in an artificial stainless-steel canal with a 60° angle and a 5-mm radius of curvature. The Reciproc M-Wire and Reciproc Blue instruments were activated with a 6:1 reduction handpiece powered by a torque-controlled motor using "RECIPROC ALL" preset program, with Reciproc Direct® contra-angle powered by an ordinary air-driven motor or with Direct® contra-angle powered by an electric motor (n = 10). The fracture surface of all fragments was examined with a scanning electron microscope. The results were statistically analyzed using Student's t test and one-way ANOVA at a significance level of P < 0.05. RESULTS: Cyclic fatigue life and number of cycles to fracture were significantly higher for Reciproc Blue instruments than for Reciproc M-Wire instruments regardless of the activation mode (P < 0.05). Instruments driven by Direct® contra-angle powered by an electric or by an ordinary air-driven motor revealed significantly longer cyclic fatigue life and number of cycles to fracture than instruments driven by an electric torque-controlled motor using "RECIPROC ALL" preset program (P < 0.05). CONCLUSIONS: Reciproc Blue instruments showed improved performance regarding fatigue resistance when compared to Reciproc M-Wire instruments. Instruments driven by Reciproc Direct® contra-angle showed higher cyclic fatigue life and number of cycles to fracture than instruments driven by an electric torque-controlled motor. CLINICAL RELEVANCE: Recently, Reciproc Direct®, the world's first contra-angle handpiece with integrated reciprocating motion, has been launched in endodontic market. The present study showed improved cyclic fatigue life of endodontic instruments when activated by Reciproc Direct®.

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AIM: The aim of this study was the assessment of the anatomical thickness of danger zone in the cervical third of mesial canals of mandibular molars. MATERIALS AND METHODS: Fifty mandibular molars were selected and scanned with cone-beam computed tomography. Data were compared using a length tool provided by scanner software. The measured areas were the mesial and distal walls of the cervical third of the mesial roots, which correspond to the safety and danger zones, respectively. In addition, dentin thickness at the furcation was evaluated. RESULTS: Dentin thicknesses of the safety zone were higher than in the danger zone in all teeth examined. The thinnest dentin of the safety zone was found at a point located 4 mm below the canal orifice, with a mean value of 1.03 mm; conversely, in the danger zone, the thinnest point was located 3 mm below the orifice, with a mean value of 0.81 mm. As for the distance from the pulp chamber floor to the furcation, the average value was 2.23 mm. CONCLUSION: These results show that mean thicknesses at the danger zone of mandibular molar mesial roots were <1.0 mm. These data reinforce the importance of understanding anatomy and the need for conservative preparations when assessing and instrumenting these root canals.

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The aim of the present study was to evaluate the cyclic fatigue of two anatomic finishing files: XP-Endo Finisher and XP-Clean. Roughness pattern and the micro-hardness of the files were also assessed. Instruments were subjected to cyclic fatigue resistance measuring the time to fracture in an artificial stainless-steel canal with a 60° angle and a 5-mm radius of curvature. The fracture surface of all fragments was examined with a scanning electron microscope. The roughness of the working parts was quantified by using a profilometer and the micro-hardness test was carried out using a Vickers hardness tester. Results were statistically analyzed using a student´s t-test at a significance level of P < 0.05. Weibull analysis was also performed. XP-Endo Finisher presented significantly longer cyclic fatigue life than XP-Clean instruments (P<0.05). XP-Endo Finisher was able to withstand 1000% more cycles to fracture when compared to XP-Clean instruments. SEM visual inspection of the fracture surfaces revealed fractographic characteristics of ductile fracture in all tested instruments; wide-ranging forms of dimples were identified and no plastic deformation in the helical shaft of the fractured instruments was observed. When mean life was compared XP-Endo Finisher lasted longer than XP-Clean with a probability of 99.9%. XP-Endo Finisher instruments also exhibited significantly lower roughness than XP-Clean instruments (P<0.05). No differences in the micro-hardness was observed between the files (P>0.05). It can be concluded that XP-Endo Finisher instruments showed improved performance when compared with XP-Clean instruments, demonstrating higher cyclic fatigue resistance and lower roughness.

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ABSTRACT Objective: This study compared the fatigue behavior of endodontic instruments manufactured with conventional NiTi alloy electropolishing, RaCe (FKG Dentaire, LaChauxdeFonds, Switzerland), with instruments manufactured with NiTi CM ​​Wire subjected to thermomechanical treatment, in the manufacturing process, HyFlex CM (Coltène Whaledent, Cuyahoga Falls, Ohio, USA), both with similar geometry and dimensions in order to determine the influence of the manufacturing process in the fatigue resistance. Methods: The methodoly consisted of twenty HyFlex CM and RaCe instruments with D0 0.25 mm, taper 0.06 mm / mm, 25 mm length, both with triangular cross section. The fracture resistance was evaluated by static fatigue test, using a stainless artificial canal with 5mm of radius (86°), recording the time and calculating the number of cycles until fracture occurs (NCF). For statistical analysis the Student t test was used The fractured instruments surface was analyzed by SEM. Results: The NCF was significantly higher for HyFlex CM instruments in comparison with RaCe files (P˂0.05) being 1336% more resistant to fatigue. The analysis of the fractured surface by SEM showed ductile-kind morphological characteristics for both instruments and the absence of plastic deformation. Conclusion: HyFlex CM instruments present higher values ​​of NCF. Thus, it can be concluded that the thermal treatment to which these instruments with CM Wire alloy are submitted makes them more resistant to fracture than Race instruments manufactured with conventional NiTi alloy electropolishing.

RESUMO Objetivo: Este estudo comparou a vida em fadiga de instrumentos endodônticos fabricados com a liga de NiTi convencional com eletropolimento de superfície, RaCe (FKG Dentaire, LaChauxdeFonds, Suiça), com instrumentos fabricados com a liga de NiTi CM Wire, submetidos a tratamento termomecânico, no processo de fabricação, HyFlex CM (Coltene Whaledent, Cuyahoga Falls, Ohio, EUA), ambos com geometria e dimensões semelhantes, visando determinar a influência do processo de fabricação das ligas e do acabamento superficial na resistência à fadiga. Métodos: Foram utilizados vinte instrumentos HyFlex CM e RaCe com D0 0,25mm, conicidade 0,06mm/mm, 25mm de comprimento, ambos com seção transversal triangular. A resistência à fratura foi avaliada através de teste estático de fadiga ciclica, utilizando um canal artificial em aço-inoxidável com 5mm de raio (86°), sendo registrado o tempo e calculado o número de ciclos para ocorrer a fratura (NCF). Para análise estatística empregou-se o teste t de Student. As superfícies de fratura dos instrumentos foram analisadas em MEV. Resultados: O NCF foi significativamente maior para os instrumentos HyFlex CM em comparação com as limas RaCe (p˂0,05), sendo 1336% mais resistentes à fadiga. A análise das superfícies fraturadas em MEV revelou características morfológicas do tipo dúctil para ambos os instrumentos e ausência de deformação plástica. Conclusão: Os instrumentos HyFlex CM apresentaram valores mais elevados de NCF. Deste modo, pode-se concluir que o tratamento térmico a qual estes instrumentos com a liga CM Wire foram submetidos os torna mais resistentes à fratura do que os instrumentos Race, fabricados com a liga de NiTi convencional com eletropolimento.

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Objetivo: esse estudo comparou a flexibilidade de instrumentos de níquel-titânio rotatórios com diferentes conicidades, em diferentes diâmetros da haste helicoidal cônica (D3 e D6). Métodos: trinta instrumentos RaCe (FKG, La Chaux-de Fonds, Suíça), #40 (D0 = 40), com 25 mm de comprimento, foram divididos em três grupos (n = 10), de acordo com sua conicidade. No teste de flexão em cantiléver (45 graus), foram realizadas duas avaliações, com cargas aplicadas, em D3 e D6, para cada grupo. Resultados: a comparação das cargas aplicadas em D3 e D6 nos instrumentos RaCe com diferentes conicidades mostrou valores de carga máxima significativamente diferentes para flexionar os instrumentos: D3 < D6, com a flexibilidade em D3 maior do que em D6. A comparação das cargas aplicadas em D3 nos três grupos revelou diferenças significativas entre os grupos (p < 0,0001), enquanto o teste Student-Newman-Keuls (SNK) mostrou diferenças de flexibilidade entre os três grupos: 0,06 < 0,04 < 0,02mm/mm. O mesmo resultado foi encontrado na comparação da força aplicada em D6. Conclusões: a flexibilidade do instrumento aumenta com a redução da conicidade (p < 0,05) e diminui com o aumento no diâmetro do eixo helicoidal (p < 0,05).

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Abstract The aim of the present study was to evaluate the cyclic fatigue of two anatomic finishing files: XP-Endo Finisher and XP-Clean. Roughness pattern and the micro-hardness of the files were also assessed. Instruments were subjected to cyclic fatigue resistance measuring the time to fracture in an artificial stainless-steel canal with a 60° angle and a 5-mm radius of curvature. The fracture surface of all fragments was examined with a scanning electron microscope. The roughness of the working parts was quantified by using a profilometer and the micro-hardness test was carried out using a Vickers hardness tester. Results were statistically analyzed using a student´s t-test at a significance level of P < 0.05. Weibull analysis was also performed. XP-Endo Finisher presented significantly longer cyclic fatigue life than XP-Clean instruments (P<0.05). XP-Endo Finisher was able to withstand 1000% more cycles to fracture when compared to XP-Clean instruments. SEM visual inspection of the fracture surfaces revealed fractographic characteristics of ductile fracture in all tested instruments; wide-ranging forms of dimples were identified and no plastic deformation in the helical shaft of the fractured instruments was observed. When mean life was compared XP-Endo Finisher lasted longer than XP-Clean with a probability of 99.9%. XP-Endo Finisher instruments also exhibited significantly lower roughness than XP-Clean instruments (P<0.05). No differences in the micro-hardness was observed between the files (P>0.05). It can be concluded that XP-Endo Finisher instruments showed improved performance when compared with XP-Clean instruments, demonstrating higher cyclic fatigue resistance and lower roughness.

Resumo O objetivo do presente estudo foi avaliar a fadiga cíclica de dois instrumentos finalizadores anatômicos: XP-Endo Finisher e XP-Clean. O padrão de rugosidade e a micro dureza dos instrumentos também foram avaliados. Os instrumentos foram submetidos à resistência à fadiga cíclica, medindo o tempo de fratura em um canal artificial de aço inoxidável com um ângulo de 60 ° e um raio de curvatura de 5 mm. A superfície de fratura de todos os fragmentos foi examinada com um microscópio eletrônico de varredura. A rugosidade dos instrumentos foi quantificada usando um perfilômetro e o teste de micro dureza foi realizado usando um testador de dureza Vickers. Os resultados foram analisados ​​estatisticamente usando o teste t de student em um nível de significância de p<0,05. A análise Weibull também foi realizada. XP-Endo Finisher apresentou vida de fadiga cíclica significativamente mais longa do que os instrumentos XP-Clean (p<0,05). XP-Endo Finisher foi capaz de suportar 1000% mais ciclos para fratura quando comparado aos instrumentos XP-Clean. A inspeção visual em microscópio eletrônico de varredura das superfícies de fratura revelou características fractográficas da fratura dúctil em todos os instrumentos testados. Não foi observada deformação plástica no eixo helicoidal dos instrumentos fraturados. Quando o tempo para a fratura foi comparado entre os instrumentos, o XP-Endo Finisher durou mais do que o XP-Clean com uma probabilidade de 99,9%. Os instrumentos XP-Endo Finisher também exibiram uma rugosidade significativamente menor do que os instrumentos XP-Clean (p<0,05). Não foram observadas diferenças na micro dureza entre os arquivos (p>0,05). Pode-se concluir que os instrumentos XP-Endo Finisher apresentaram desempenho melhorado em comparação com os instrumentos XP-Clean, demonstrando maior resistência à fadiga cíclica e menor rugosidade.

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OBJECTIVE: To propose bismuth carbonate, a radiopacifying agent, as a new endodontic root repair material that was added to Portland cement (PC) at 2 wt%, 5 wt%, 10 wt% and 15 wt%, and physicochemical and biological properties of each formulation were evaluated in comparison to MTA-Angelus. METHODS: Mixed and powder samples were analysed by scanning electron microscopy (SEM) and X-ray power diffraction (XRD), and the semiquantitative constitution of the powder was determined by energy-dispersive spectrometer (EDS). Setting time was evaluated by Vicat needle and radiopacity analysed with digital X-ray. The pH of all tested materials was observed after immersion in water for 3, 24, 48, 72 and 168 h (or 7 days). Solubility and calcium release were measured after immersion in water for 24 h. A multiparametric assay XTT-NR-CVDE was used to evaluate the cytotoxicity of the materials in human periodontal ligament (HPDL) fibroblasts. HPDL fibroblasts were exposed to PC 15% and mineral trioxide aggregate (MTA), and the expression of proinflammatory cytokines (IL1A, IL6, IL8, TNF) and bone formation genes (ALP, COL1, RUNX2) was evaluated by real-time PCR. Mineralisation of HPDL fibroblasts cocultured with PC, PC 15% and MTA was evaluated with Von Kossa staining. RESULTS: PC-based groups presented more irregular and larger particles than MTA. PC and MTA showed similarities as observed by XRD and EDS. Setting time of PC-based groups was increased with the addition of bismuth carbonate. All tested materials were alkaline, and pH tended to reduce over time. All cements had solubility lower than recommended, with no difference between them (P>0.05) and showed calcium release. PC 15% had similar radiopacity when compared with MTA (P>0.05). Cell viability was higher for the tested materials than the positive control (P<0.001), but there was no difference when they were compared with negative control (P>0.05). Gene expression levels were similar for all tested groups (P>0.05). Analysed cements had positive Von Kossa staining. CONCLUSION: Overall, the addition of 15% of bismuth carbonate did not result in significant changes to its physicochemical and biological properties when compared with MTA, except for the setting time, and may be considered a potential substitute for MTA.

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Objetivo: esse estudo teve como objetivo avaliar a resistência à fratura por torção de duas marcas de instrumentos mecanizados de NiTi, com formas geométricas distintas e produzidas por ligas metálicas diferentes. Métodos: quinze instrumentos WaveOne Large e quinze ProTaper F4 foram selecionados e submetidos aos ensaios mecânicos de torção, microdureza Vickers e tenacidade. No ensaio de torção, foram avaliados a deformação angular até a fratura e o torque máximo. As superfícies fraturadas e as hastes helicoidais dos instrumentos foram analisadas por meio de microscopia eletrônica de varredura (MEV). Resultados: os valores do ângulo máximo em torção foram maiores para o ProTaper, enquanto o torque máximo em torção (N/cm) foi maior para o WaveOne. Os valores de microdureza Vickers foram maiores para a liga NiTi M-Wire, enquanto o grupo controle apresentou maior tenacidade. O teste t de Student demonstrou diferença significativa nos ensaios de torção (p < 0,05), tenacidade e microdureza Vickers. A análise do MEV revelou deformação plástica ao longo das hélices helicoidais de todos os instrumentos fraturados e fratura tipo dúctil. Conclusão: os instrumentos fabricados em NiTi M-Wire apresentaram maior resistência à fratura por torção e maior microdureza, em comparação aos de NiTi convencional. Devido ao maior ângulo de torção do ProTaper e à maior deformação até a fratura, esses parâmetros tornam esse instrumento mais seguro do ponto de vista clínico.

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Introduction: Cervical preflaring is an important step of the canal system instrumentation, but can lead to excessive enlargement or root perforation. Objective: Evaluate the remaining dentin thickness in the mandibular molars of mesial roots using cone beam computed tomography: Gates-Glidden (crown-down); Gates-Glidden (step-back); LA Axxess and Easy Pro-Design. Material and method: Were selected 40 lower molars mesial roots, which were scanned in a cone beam CT scanner before and after preparation. Were obtained five sections of the CT images with an interval of 1 mm from the furcation, and measured the thickness variation between the root canal to the root external portion in analysis software. Result: The evaluation of the different levels showed no significance within the same group for the Gates-Glidden group. On the other hand, were observed difference for LA Axxess (p=0.002) and Easy Pro-Design (p=0.005). In the intergroup analysis, were observed difference in all levels, especially for Gates-Glidden in the ascendant order (ANOVA and Tukey). Conclusion: Within the limitations of these study, is possible to conclude that the protocol with greater wear in the cervical risk area was the Gates-Glidden in step-back sequence, as the other groups were equivalent (p>0.05).

Introdução: O preparo cervical é uma etapa importante da instrumentação do sistema de canais, mas pode levar ao alargamento excessivo ou rasgo da raiz. Objetivo: Avaliar, em tomografia computadorizada cone beam, da espessura remanescente de dentina cervical da raiz mesial de molares inferiores, após o preparo com diferentes técnicas: Gates-Glidden (ordem crescente); Gates-Glidden (ordem decrescente); LA Axxess e Easy Pro-Design. Material e método: Foram selecionadas 40 raízes mesiais de molares inferiores, que foram escaneadas em tomógrafo cone beam antes e após o preparo. Das imagens tomográficas foram obtidos cinco cortes com intervalo de 1 mm a partir da furca e, então, mensurada a variação da espessura entre o canal radicular até a porção externa da raiz em software de análise. Resultado: Avaliação dos diferentes níveis demonstraram ausência de significância dentro do mesmo grupo para o grupo das Gates-Glidden. Por outro lado, foi notada diferença para LA Axxess (p=0,002) e para Easy Pro-Design (p=0,005). Na avaliação entre os grupos, foi observada diferença em todos os níveis, sobretudo, para Gates-Glidden na ordem crescente (ANOVA e Tukey). Conclusão: Considerando as limitações desse estudo, concluiu-se que o protocolo que apresentou maior desgaste da área de perigo cervical foi o da Gates-Glidden em ordem crescente, sendo que os demais grupos foram equivalentes (p>0,05).

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