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1.
J Prosthodont ; 33(4): 389-395, 2024 Apr.
Artigo em Inglês | MEDLINE | ID: mdl-37201944

RESUMO

PURPOSE: This study evaluated the fatigue failure load (FFL) and the number of cycles for fatigue failure (CFF) of traditional (porcelain layer up) and reversed (zirconia layer up) designs of porcelain-veneered zirconia samples prepared with heat-pressing or file-splitting techniques. MATERIALS AND METHODS: Zirconia discs were prepared and veneered with heat-pressed or machined feldspathic ceramic. The bilayer discs were bonded onto a dentin-analog according to the bilayer technique and sample design: traditional heat-pressing (T-HP), reversed heat-pressing (R-HP), traditional file-splitting with fusion ceramic (T-FC), reversed file-splitting with fusion ceramic R-FC), traditional file-splitting with resin cement (T-RC), and reversed file-splitting with resin cement (R-RC). The fatigue tests were performed using the stepwise approach at 20 Hz, 10,000 cycles/step, step-size of 200 N starting at 600 N, and proceeding until failure detection or up to 2600 N if enduring. The failure modes (from radial and/or cone cracks) were analyzed in a stereomicroscope. RESULTS: The reversed design decreased the FFL and CFF of bilayers prepared with heat-pressing and file-splitting with fusion ceramic. The T-HP and T-FC reached the highest results, which were statistically similar between them. The bilayers prepared by the file-splitting with resin cement (T-RC and R-RC) were similar to the R-FC and R-HP groups regarding FFL and CFF. Almost all reverse layering samples failed by radial cracks. CONCLUSIONS: The reverse layering design did not improve the fatigue behavior of porcelain veneered zirconia samples. The three bilayer techniques behaved similarly when used in the reversed design.


Assuntos
Cerâmica , Porcelana Dentária , Cerâmica/uso terapêutico , Cerâmica/química , Porcelana Dentária/química , Coroas , Cimentos de Resina , Teste de Materiais , Propriedades de Superfície , Análise do Estresse Dentário , Zircônio/química , Falha de Restauração Dentária
2.
Braz. j. oral sci ; 21: e224265, jan.-dez. 2022. tab
Artigo em Inglês | LILACS, BBO - Odontologia | ID: biblio-1354719

RESUMO

Aim: This study assessed the color and translucency stability of a polymer infiltrated ceramic network (PICN) and compared it with a resin composite (RC) and a feldspathic ceramic (FEL). Methods: Disc-shaped samples of a PICN (Vita Enamic), a feldspathic ceramic (Vitablocks Mark II), and a resin composite (Brava block) were prepared from CAD/CAM blocks. PICN and RC surfaces were finished with a sequence of polishing discs and diamond paste. FEL samples received a glaze layer. The samples were subjected to 30-min immersions in red wine twice a day for 30 days. CIEL*a*b* coordinates were assessed with a spectrophotometer at baseline and after 15 and 30 days of immersion. Color alteration (ΔE00) and translucency parameter (TP00) were calculated with CIEDE2000. Average roughness was measured before the staining procedures. Color difference and translucency data were analyzed with repeated-measures ANOVA and Tukey's tests. Roughness was analyzed with the Kruskal-Wallis test. Results: Roughness was similar among the experimental groups. All materials had their color alteration significantly increased from 15 to 30 days of staining. PICN reached an intermediate ΔE00 between FEL and RC at 15 days. PICN revealed a color alteration as high as the composite after 30 days. No statistical difference was observed regarding translucency. Conclusion: PICN was not as color stable as the feldspathic ceramic at the end of the study. Its color alteration was comparable to the resin composite when exposed to red wine. However, the translucency of the tested materials was stable throughout the 30-day staining


Assuntos
Propriedades de Superfície , Teste de Materiais , Cerâmica , Desenho Assistido por Computador , Cor , Resinas Compostas
3.
Clin Oral Investig ; 26(6): 4479-4486, 2022 Jun.
Artigo em Inglês | MEDLINE | ID: mdl-35435492

RESUMO

OBJECTIVE: The aim of this study was to evaluate the effect of four different finishing procedures on the fatigue strength of a fully stabilized zirconia (5Y-FSZ) material. MATERIALS AND METHODS: Disc-shaped specimens of a 5Y-FSZ (Katana UTML, Kuraray Noritake) were made (ISO 6872-2015), grinded with 600- and 1200-grit silicon carbide paper, sintered as recommended, and randomly assigned into four groups according to the finishing technique: C (control, as-sintered), P (polished with polishing rubbers), G (glaze application - powder/liquid technique), and PG (polished with polishing rubbers + glaze application - powder/liquid). Then fatigue strength (staircase method), X-ray diffraction (XRD), and scanning electron microscopy (SEM) analyses were performed. RESULTS: The C group presented the lowest fatigue strength, while the PG group presented the highest. The P and G groups presented intermediate behavior, presenting similar statistical results. XRD showed similar crystalline phase patterns for all groups. SEM images revealed some changes in the zirconia surface, with the P group presenting some scratches on the surface, while the scratches in the PG group were filled with the glaze material. CONCLUSION: None of the techniques analyzed in this study impaired the fatigue strength of fully stabilized zirconia. Importantly, the polishing rubbers combined with glaze application (PG group) improved its fatigue strength. CLINICAL RELEVANCE: The polishing rubbers followed by glaze application improve the fatigue strength in ultra-translucent zirconia.


Assuntos
Teste de Materiais , Zircônio , Cerâmica/química , Polimento Dentário , Humanos , Microscopia Eletrônica de Varredura , Pós , Propriedades de Superfície , Zircônio/química
4.
J Prosthodont Res ; 64(1): 12-19, 2020 Jan.
Artigo em Inglês | MEDLINE | ID: mdl-31213364

RESUMO

PURPOSE: To characterize the effect of two processing techniques (pressing and CAD/CAM - Computer Aided Design/Computer Aided Machining) of lithium-disilicate (LD) based crowns on the microstructure, topography, roughness, fractal dimension, internal and marginal adaptation. METHODS: One-hundred identical preparations for monolithic crowns were made with dentin analogue material (G10 epoxy resin). One of the preparations was scanned and a monolithic crown in lithium-disilicate was planned in the CAD system. Fifty crowns were milled in a wax pattern and subjected to pressing (IPS e.max Press), while 50 crowns were machined at CAD/CAM (IPS e.max CAD) and posteriorly crystallized. Internal and marginal adaptation were assessed via replica technique at four manufacturing moments (Milled wax pattern; LDPRESS; Milled LDCAD; Crystallized LDCAD) and considering 5 regions (margin, cervico-axial angle, axial wall, axial-occlusal angle and occlusal wall). Complementary analysis considering microstructure and topography, roughness and fractal dimension were performed in Scanning Electron Microscopy (SEM) and Atomic Force Microscopy (AFM). RESULTS: The processing technique resulted in different ceramic microstructure, topography, roughness and fractal dimension, whereas CAD/CAM lead to smoother, more homogeneous but more complex topography features (higher fractal dimension) in comparison to the pressing technique (P<0.05). Regarding marginal and internal fit, LDPRESS crowns showed to be more adapted at the margin, while LDCAD were more adapted at the occluso-axial angle; other regions were not statistically different (α=0.05). CONCLUSIONS: CAD/CAM and the pressing techniques for manufacturing LD crowns lead to completely different ceramic surface characteristics and affect crown adaptation at the margin and at occluso-axial angle.


Assuntos
Adaptação Marginal Dentária , Lítio , Cerâmica , Desenho Assistido por Computador , Coroas , Técnica de Fundição Odontológica , Técnica de Moldagem Odontológica , Porcelana Dentária , Planejamento de Prótese Dentária , Fractais , Propriedades de Superfície
5.
J Mech Behav Biomed Mater ; 91: 122-130, 2019 03.
Artigo em Inglês | MEDLINE | ID: mdl-30579109

RESUMO

The present study evaluated the fatigue behavior of monolithic translucent zirconia polycrystals (TZ) and lithium disilicate glass-ceramic (LD) bonded to different substrates. Disc-shaped specimens of ceramic materials TZ and LD were bonded to three substrates with different elastic modulus (E) (fiber-reinforced composite (FRC) - softest material, E = 14.9 GPa; titanium alloy (Ti) - intermediary properties, E = 115 GPa; and zirconia (Yz) - stiffest material, E = 210 GPa). The surfaces were treated and bonded with resin cement (disc-disc set-up). Fatigue testing followed a step-stress approach (initial maximum load = 200 N for 5000 cycles, incremental step load = 200 N for 10,000 cycles/step). The fatigue failure load and number of cycles until failure were recorded and statistically analyzed. Fractographic and finite element (FEA) analyzes were conducted as well. TZ ceramic depicted higher fatigue failure load, number of cycles until failure, and survival probabilities than LD, irrespective of the substrate. Moreover, TZ and LD presented better fatigue behaviors when bonded to substrates Ti and Yz in comparison to FRC. FEA revealed lower tensile stresses at restorative material when bonded to stiffer substrates. Fractography showed that the fracture origin started at bottom surface of restorative material (except for TZ bonded to Yz, in which crack initiated at load contact point). Translucent zirconia polycrystals present superior mechanical behavior than lithium disilicate glass-ceramic. The substrate type influences the mechanical performance of monolithic dental ceramics (stiffer substrates lead to better fatigue behavior).


Assuntos
Cerâmica/química , Colagem Dentária , Porcelana Dentária/química , Teste de Materiais , Zircônio/química , Análise de Elementos Finitos , Estresse Mecânico , Suporte de Carga
6.
Braz Dent J ; 29(5): 483-491, 2018.
Artigo em Inglês | MEDLINE | ID: mdl-30517448

RESUMO

It evaluated the effect of aging by Low Temperature Degradation (LTD), executed after post- processing surface treatments (polishing, heat treatment and glazing), on the surface characteristics (micromorphology and roughness) and on the structural stability (phase transformation and mechanical behavior-flexural strength and structural reliability) of a ground yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) ceramic. Discs of Y-TZP (VITA In-Ceram YZ) were manufactured (ISO:6872-2015; 15 mm in diameter and 1.2 ± 0.2 mm in thickness) and randomly assigned into 10 groups according two factors: "aging" in 2 levels (with or without) and "surface treatment" in 5 levels (Ctrl: as-sintered; Gr: grinding with coarse diamond bur; Gr + HT: grinding plus heat treatment; Gr + Pol: grinding plus polishing; Gr + Gl: grinding plus glazing). Roughness (n=30), biaxial flexural test (n=30), phase transformation (n=2), and surface topography (n=2) analyses were performed. Aging led to an intense increase in monoclinic (m) phase content for all the tested conditions, being the as-sintered samples (Ctrl= 65.6%) more susceptible to the t-m phase transformation. Despite of increasing the m-phase content, aging was not detrimental for characteristic strength (except to the grinding condition). There was no significant reduction in the Weibull modulus after surface treatments. Additionally, heat treatment and glazing after grinding led to a decrease in characteristic strength, while polishing presented the highest characteristic strength values. Thus, polishing is mandatory after grinding the Y-TZP ceramic, while performing glazing or heat-treatment alone after grinding lead to the worst mechanical performance.


Assuntos
Materiais Dentários/química , Polimento Dentário/métodos , Ítrio/química , Zircônio/química , Resistência à Flexão , Temperatura Alta , Teste de Materiais , Microscopia de Força Atômica , Microscopia Eletrônica de Varredura , Propriedades de Superfície , Difração de Raios X
7.
Braz. dent. j ; 29(5): 483-491, Sept.-Oct. 2018. tab, graf
Artigo em Inglês | LILACS | ID: biblio-974179

RESUMO

Abstract It evaluated the effect of aging by Low Temperature Degradation (LTD), executed after post- processing surface treatments (polishing, heat treatment and glazing), on the surface characteristics (micromorphology and roughness) and on the structural stability (phase transformation and mechanical behavior-flexural strength and structural reliability) of a ground yttrium-stabilized tetragonal zirconia polycrystal (Y-TZP) ceramic. Discs of Y-TZP (VITA In-Ceram YZ) were manufactured (ISO:6872-2015; 15 mm in diameter and 1.2 ± 0.2 mm in thickness) and randomly assigned into 10 groups according two factors: "aging" in 2 levels (with or without) and "surface treatment" in 5 levels (Ctrl: as-sintered; Gr: grinding with coarse diamond bur; Gr + HT: grinding plus heat treatment; Gr + Pol: grinding plus polishing; Gr + Gl: grinding plus glazing). Roughness (n=30), biaxial flexural test (n=30), phase transformation (n=2), and surface topography (n=2) analyses were performed. Aging led to an intense increase in monoclinic (m) phase content for all the tested conditions, being the as-sintered samples (Ctrl= 65.6%) more susceptible to the t-m phase transformation. Despite of increasing the m-phase content, aging was not detrimental for characteristic strength (except to the grinding condition). There was no significant reduction in the Weibull modulus after surface treatments. Additionally, heat treatment and glazing after grinding led to a decrease in characteristic strength, while polishing presented the highest characteristic strength values. Thus, polishing is mandatory after grinding the Y-TZP ceramic, while performing glazing or heat-treatment alone after grinding lead to the worst mechanical performance.


Resumo Este estudo avaliou o efeito do envelhecimento através da degradação a baixas temperaturas (low temperaturare degradation - LTD) após a realização de tratamentos de superfície pós- sinterização (polimento, tratamento térmico e glaze) nas características superficiais (micromorfologia e rugosidade), e na estabilidade estrutural (transformação de fase e comportamento mecânico - resistência flexural e confiabilidade estrutural) de uma cerâmica de zircônia tetragonal policristalina estabilizada por ítria (Y-TZP) desgastada. Discos de cerâmica Y-TZP (VITA In-Ceram YZ) foram confeccionados (ISO:6872-2015; 15mm de diâmetro e 1,2 ± 0,2mm de espessura) e randomicamente divididos em 10 grupos de acordo com dois fatores: "envelhecimento" (com e sem) e "tratamento de superfície" (Ctrl - sem tratamento; Gr - desgaste com ponta diamantada grossa; Gr + HT - desgaste mais tratamento térmico; Gr + Pol - desgaste mais polimento; Gr + Gl - desgaste mais glazeamento). Foram realizadas as análises de rugosidade (n=30), flexão biaxial (n=30), transformação de fase (n=2) e topografia de superfície (n=2). O envelhecimento levou a um aumento intenso no conteúdo de fase monoclínica (m) em todas as condições testadas, sendo observada uma maior susceptibilidade de transformação de fase t-m nas amostras do grupo controle (Ctrl= 65.6%). Apesar de provocar elevada transformação de fase, o envelhecimento não apresentou efeitos negativos nos desfechos avaliados. Não houve redução significativa do módulo de Weibull após os tratamentos. Além disso, o tratamento térmico e o glaze após desgaste levaram a uma redução da resistência característica, enquanto que o grupo polimento apresentou o mais alto valor de resistência característica. O glaze e o tratamento térmico geraram o pior desempenho mecânico, portanto a realização do polimento após desgaste de uma cerâmica Y-TZP é obrigatória.


Assuntos
Ítrio/química , Zircônio/química , Materiais Dentários/química , Polimento Dentário/métodos , Propriedades de Superfície , Difração de Raios X , Teste de Materiais , Microscopia Eletrônica de Varredura , Microscopia de Força Atômica , Resistência à Flexão , Temperatura Alta
8.
Rev. cir. traumatol. buco-maxilo-fac ; 15(3): 7-13, Jul.-Set. 2015. tab
Artigo em Português | LILACS, BBO - Odontologia | ID: lil-792387

RESUMO

A lavagem das mãos reduz as bactérias da pele, diminuindo as taxas de infecções. Há várias técnicas de higienização das mãos, devendo o profissional escolher a mais adequada. OBJETIVOS: este trabalho avaliou a eficácia da lavagem cirúrgica das mãos e antebraços com escova impregnada com clorexidina a 2%, comparando com o método de fricção das mãos e antebraço com sabonete líquido contendo clorexidina a 2%. MATERIAIS E MÉTODOS: foram analisadas amostras das pontas dos dedos polegar e indicador, palma da mão e antebraço, de 40 alunos do curso de Odontologia da UNIFRA. A primeira degermação realizada foi com a escova impregnada com clorexidina a 2%, e, sete dias após, os mesmos participantes degermaram as mãos com sabonete contendo clorexidina a 2%. As amostras foram coletadas em placas contendo meio Ágar Base Sangue, identificadas e levadas ao laboratório de microbiologia. RESULTADOS:os mostraram que o método de fricção com sabonete contendo clorexidina a 2% apresentou melhores resultados. CONCLUSÃO: a higienização das mãos pelo método de fricção com sabonete contendo clorexidina a 2% foi mais eficaz quando comparada à realizada com escova impregnada com clorexidina a 2%, sugerindo um método de preparo pré-cirúrgico das mãos mais rápido, eficaz e menos oneroso... (AU)


ABSTRACT Hand washing reduces the amount of skin bacteria, thus contributing to reducing infection rates. There are several techniques for hand washing and the health professional should choose the most appropriate one. OBJECTIVES: This study evaluated the effectiveness of surgical hands and forearms washing made with brush impregnated with 2% chlorhexidine, compared with the friction method of hands and forearms with liquid soap containing 2% chlorhexidine. MATERIALS AND METHODS: We analyzed tip of the thumb and index finger, palm and forearm from 40 students of Dentistry from UNIFRA. The first protocol antisepsis was performed with a brush impregnated with 2% chlorhexidine, and seven days later, the same participants washed their hands with soap containing 2% chlorhexidine. The samples were collected in plates containing Blood Agar Base, identified and taken to the microbiology laboratory. RESULTS:The method of rubbing the soap containing 2% chlorhexidine performed better. CONCLUSION: Hand hygiene by friction method with soap containing 2% chlorhexidine is more effective than the one performed with brush impregnated with 2% chlorhexidine, suggesting a faster, effective and less costly presurgical hand preparation... (AU)


Assuntos
Humanos , Procedimentos Cirúrgicos Operatórios , Clorexidina , Desinfecção das Mãos , Controle de Infecções , Higiene das Mãos , Bactérias , Indicadores e Reagentes , Fenômenos Microbiológicos
9.
RSBO (Impr.) ; 11(1): 100-106, Jan.-Mar. 2014. ilus
Artigo em Inglês | LILACS | ID: lil-718014

RESUMO

Introduction: Severe early childhood caries (S-ECC) is very common in pre-school children and shows a pattern of development which is defined and symmetrical, beginning on the cervical third of labial surface of maxillary anterior teeth. Accordingly, it can damage speech, swallowing, feeding, development, esthetics and self-esteem of the child. Objective: To report a case of a 5-year-old female patient with S-ECC on teeth #51, #52, #61 and #62. Case report: The patient came to dental clinic of the university with her mother for dental care. During the interview, the mother reported that her daughter used to drink milk in baby bottle at day and night with sugar content. Moreover, oral hygiene was not performed after bottle feeding at night. On clinical examination, the teeth #51, #52, #61 and #62 presented coronal destruction, and the mucosa associated at these teeth was very inflamed. Radiographically, it was found that carious lesions were limited to inner dentin. The treatment plan included education on oral hygiene and diet guidance. Rehabilitation with acetate matrixes was the treatment chosen for teeth destroyed by caries. Conclusion: This study demonstrated that the use of acetate matrixes is an effective alternative to return aesthetics and functionality to teeth of patients with severe early childhood caries.

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